Difference between revisions of "Crystallisation and precipitation"
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{{Infobox technology|Category=[[Pre-processing]] ([[Pre-processing#Separation_technologies|Separation technologies]]), [[Post-processing]] ([[Post-processing#Separation_technologies|Separation technologies]])|Name=Crystallisation and precipitation}} | {{Infobox technology|Category=[[Pre-processing]] ([[Pre-processing#Separation_technologies|Separation technologies]]), [[Post-processing]] ([[Post-processing#Separation_technologies|Separation technologies]])|Name=Crystallisation and precipitation}} | ||
<onlyinclude>[[File:NaCl octahedra and part of crystal.svg|alt=Graphic showing NaCl (table salt) crystal consisting of sodium and chlorine atoms|thumb|200x200px|NaCl (table salt) crystal consisting of sodium and chlorine atoms | <onlyinclude>[[File:NaCl octahedra and part of crystal.svg|alt=Graphic showing NaCl (table salt) crystal consisting of sodium and chlorine atoms|thumb|200x200px|NaCl (table salt) crystal consisting of sodium and chlorine atoms]]'''Crystallisation''' is the formation of crystals from a solution. In a crystal, the atoms or molecules are highly organised into a solid repetitive structure. A simple example for crystallisation is the evaporation of the solvent. For example the salinity of the Great Salt Lake in Utah, USA, is so high that through the evaporation of water salt crystals cover its shores. Some other ways in which crystals form are precipitating from a solution, freezing, or more rarely deposition directly from a gas. Attributes of the resulting crystal depend largely on factors such as temperature, air pressure, and in the case of liquid crystals, time of fluid evaporation.</onlyinclude> | ||
==Feedstock== | ==Feedstock== |
Revision as of 14:15, 21 February 2022
Technology | |
Technology details | |
Name: | Crystallisation and precipitation |
Category: | Pre-processing (Separation technologies), Post-processing (Separation technologies) |
Feedstock: | |
Product: |
Crystallisation is the formation of crystals from a solution. In a crystal, the atoms or molecules are highly organised into a solid repetitive structure. A simple example for crystallisation is the evaporation of the solvent. For example the salinity of the Great Salt Lake in Utah, USA, is so high that through the evaporation of water salt crystals cover its shores. Some other ways in which crystals form are precipitating from a solution, freezing, or more rarely deposition directly from a gas. Attributes of the resulting crystal depend largely on factors such as temperature, air pressure, and in the case of liquid crystals, time of fluid evaporation.
Feedstock
Origin and composition
Pre-treatment
Process and technologies
Crystallization occurs in three major steps. The first is nucleation, the appearance of a crystalline phase from either a supercooled liquid or a supersaturated solvent. The second step is known as crystal growth, which is the increase in the size of particles and leads to a crystal state. An important feature of this step is that loose particles form layers at the crystal's surface and lodge themselves into open inconsistencies such as pores, cracks, etc.
The majority of minerals and organic molecules crystallize easily, and the resulting crystals are generally of good quality, i.e. without visible defects. However, larger biochemical particles, like proteins, are often difficult to crystallize. The ease with which molecules will crystallize strongly depends on the intensity of either atomic forces (in the case of mineral substances), intermolecular forces (organic and biochemical substances) or intramolecular forces (biochemical substances).
Crystallization is also a chemical solid–liquid separation technique, in which mass transfer of a solute from the liquid solution to a pure solid crystalline phase occurs. In chemical engineering, crystallization occurs in a crystallizer. Crystallization is therefore related to precipitation, although the result is not amorphous or disordered, but a crystal.
Products
Post-treatment
Technology providers
Company name | Country | Technology category | Technology name | TRL | Capacity [kg/h] | Processable volume [L] | Feedstock: Food waste | Feedstock: Garden & park waste |
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Company 1 | [Country HQ location] | [Technology category (if different sub-categories are defined this has to be specified here, the available categories can be found on each technology page under the chapter Process and technologies)] | [Technology name (the "branded name" or the usual naming from company side)] | [4-9] | [numeric value] | ● | ● | |
Company 2 | [Country HQ location] | [(if different sub-categories are defined this has to be specified here, the available categories can be found on each technology page under the chapter Process and technologies)] | [Technology name (the "branded name" or the usual naming from company side)] | [4-9] | [numeric value] | ● | ● |
ABC
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Technology name: | Technology category: | Pre-processing (Separation technologies), Post-processing (Separation technologies) | |
TRL: | Capacity: | kg·h-1 | |
Agitator: | Processable volume: | L | |
Reactor: | Reactor material: | ||
Separation type: | Other: | ||
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Feedstock: | Product: |
describe the company, here is an example
ABC was founded in 20... 12 by KNN and Syncom, in collaboration with the university of Groningen, Netherlands. The company is a technology provider developing chemical recycling technologies for different feedstocks including non-food bio- and plastics waste. In 2018 a pilot plant with the capability to process biomass and plastic waste was set up at the Zernike Advanced Processing (ZAP) Facility. The company is now focused on setting up their first commercial plant with a capacity of 20,000 to 30,000 tonnes. The investing phase B was recently completed, with the last investment phase in 2019 the financial requirements are fulfilled to complete the commercialisation activities to build the plant which is expected for 2023.
describe their technology, here is an example
The technology is based on an Integrated Cascading Catalytic Pyrolysis (ICCP) process, being able to produce aromatics including benzene, toluene, and xylene (BTX) as well as light olefins from low grade biomass and plastics waste. This technology utilises catalytic cracking in a two-step process at temperatures between 450- 850 °C. In the first step the feedstock material is vaporised via thermal cracking. The pyrolysis vapours are then directly passed into a second reactor in which they are converted into aromatics by utilising a zeolite catalyst which can be continuously regenerated. Finally, the products are separated from the gas via condensation. An ex situ approach of catalytic conversion has several advantages such as the protection of the catalyst from deactivation/degradation expanding its lifetime, a greater variety of feedstock, and a precise adjustment of process conditions (e.g. temperature, catalyst design, and Weight Hourly Space Velocity (WHSV) in each step for improved yields. In current pilot plant with 10 kg h-1 feed capacity for either waste plastics or biomass, final design details are established, which will be include in the running engineering activities for the commercial plant.
Open access pilot and demo facility providers
Patents
Currently no patents have been identified.