Difference between revisions of "Ultrasonication"

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== Technology providers ==
== Technology providers ==
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|+'''Technology comparison'''
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Company name
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Company name
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Country
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Country
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Technology category
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Technology subcategory
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Technology name
! class="cd-text-darkgreen" style="vertical-align:{{{va|bottom}}}"| Technology name
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| [[Help:Article content of technology pages#Company_1|Company 1]]
| [[Ultrasonication#Everywave Srl|Everywave Srl]]
| [Country HQ location]
| Italy
| [Technology category (if different sub-categories are defined this has to be specified here, the available categories can be found on each technology page under the chapter [[Help:Article content of technology pages#Process_and_technologies|Process and technologies]])]
| -
| [Technology name (the "branded name" or the usual naming from company side)]
| FLOW:WAVE® Tubular reactor
| [4-9]
| 5
| [numeric value]
| 2000
|
|20-40
|
|2000-4000
|
|4
|
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
|-
| [[Ultrasonication#Hielscher Ultrasonics GmbH|Hielscher Ultrasonics GmbH]]
| Germany
| -
| UIP16000
| 9
| -
|18
|40000
|5
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
|-
|[[Ultrasonication#Doosan Enpure Limited|Doosan Enpure Limited]]
|United Kingdom
| -
|SonixTM
| -
| -
|20
| -
| -
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
|-
|-
| [[Help:Article content of technology pages#Company_2|Company 2]]
|[[Ultrasonication#Ultrawaves|Ultrawaves]]
| [Country HQ location]
|Germany
| [(if different sub-categories are defined this has to be specified here, the available categories can be found on each technology page under the chapter [[Help:Article content of technology pages#Process_and_technologies|Process and technologies]])]
| -
| [Technology name (the "branded name" or the usual naming from company side)]
|BIOSONATOR
| [4-9]
| -
| [numeric value]
|1980
|
|20-1000
|
|10000
|
|20-50
|
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
|-
|[[Ultrasonication#VTA|VTA]]
|Austria
| -
|VTA GSD
| -
| -
|25
|3000-4000
|300-2500
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
|-
|[[Ultrasonication#Weber|Weber]]
|Germany
| -
|DesiUS/BIOPUSH
|9
| -
|22
|2000
| -
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| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
| class="cd-background-lightgreen cd-text-darkgreen" style="text-align:center" |●
|}
|}
=== Company 1 ===
 
{{Infobox provider-ultrasonication}}
=== Everywave Srl ===
{{Infobox provider-ultrasonication|Company=Everywave Srl|Contact=info@everywave.eu|Country=Italy|Webpage=https://www.everywave.eu/en/|TRL=5|Technology name=FLOW:WAVE® Tubular reactor|Power=2000/4000|Other=Continuous process|Frequency=20/40|Processable volume=4|Product=emulsion, mixing, disintegration, sonochemistry, plant extraction, and bactericidal action.|Feedstock=By-products and biomasses (slurry, manure, sorghum, triticale, corn silage, other livestock waste, or residues from the agri-food industry, etc.)|Image=Everywavelogo.png|Capacity=2 tons/hour per single module}}
Everywave Srl is a spin-off from UNITECH Srl that specializes in the research, development and production of solutions in the ultrasound technologies. The continuous and rapid technological evolution and the need for ever higher quality standards require the daily research and development of increasingly innovative solutions where quality and reliability play an absolutely vital role in all working processes. Everywave’s mission has always been to find ideas and improvement solutions in the field of ultrasound technologies, with continuous support to its customers in order to optimize their productivity and therefore their competitiveness.
 
Today, with a specialized biomass treatment plant, the company also produces biogas from the same by-products: a source that reduces the energy supply costs necessary for the company and generates a new source of income. We have designed and produced a special ultrasonic reactor which, integrated with specialized systems for shredding, pumping and process control, represents a solid and efficient technology for controlling and increasing the production yield of biogas.


=== Hielscher Ultrasonics GmbH ===
=== Hielscher Ultrasonics GmbH ===
{{Infobox provider-ultrasonication|Company=Hielscher Ultrasonics GmbH|Contact=info@hielscher.com|Country=Germany|Webpage=www.hielscher.com|TRL=9|Technology name=UIP16000|Power=40,000|Other=Biodiesel transesterification (12-50m³/h ) Emulsification (e.g. oil/water 6-32m³/h), Cell extraction (e.g. algae 1-12m³/h), Dispersion/deagglomeration (0.3-6m³/h), Wet milling (0.2-4m³/h)|Frequency=18|Processable volume=5|Product=Dispersion, Emulsion, Cell extract|Feedstock=Biomass, 2-phase systems|Image=Hielscher.png}}
Hielscher Ultrasonics specialises in the design and manufacturing of high power ultrasonic homogenisers for lab, bench-top and production level. Ultrasonic power is an effective and energy-efficient means to apply high shear and intense stress to liquids, powder/liquid mixtures and slurries. This makes it a strong alternative to high shear mixers, high pressure homogenisers and agitated bead mills. Hielscher ultrasonic devices are in use worldwide as laboratory mixers, high shear mixing equipment, full-size in-line homogenisers or particle mills. The applications include mixing, dispersing, particle size reduction, extraction and chemical reactions. Hielscher supply to various industry segments, such as nano-materials, paints & pigments, food & beverage, cosmetics, chemicals and fuels.
=== Doosan Enpure Limited ===
{{Infobox provider-ultrasonication|Company=Doosan Enpure Limited|Country=United Kingdom|Webpage=https://www.doosanenpure.com/|Technology name=SonixTM|Frequency=20|Product=Disintegrated material|Feedstock=Wastewater sludge, or any other biological or cellular material|Capacity=200 m3/d}}
Doosan Enpure Limited is a process engineering company specializing in water, wastewater and sludge treatment as well as waste-to-energy solutions with a global presence. We are a wholly-owned subsidiary of Doosan Heavy Industries & Construction, a global conglomerate in the power and water infrastructure sector, headquartered in South Korea.
Doosan Enpure provides a wide range of sludge treatment processes to meet all legislative requirements as well as maximising the recovery of energy and other useful components of the sludge.
=== Ultrawaves ===
{{Infobox provider-ultrasonication|Company=ULTRAWAVES - Water- and Environmental Technologies GmbH|Country=Germany|Webpage=https://ultrawaves.de/en/|Technology name=BIOSONATOR|Power=3000-10000|Frequency=20-1000|Processable volume=20-50|Product=Disintegrated biomass for further processing|Feedstock=Renewable raw materials, maize, green waste, slurry, municipal and industrial wastewater|Capacity=10 to 33 L/min or 0.6 to 2 m3/h biomass suspension}}
ULTRAWAVES GmbH develops and markets innovative high-power ultrasonic systems for water and environmental engineering. Apart from the disintegration of biomass in wastewater treatment and biogas plants, the systems are also used in industrial applications. In 2001 Ultrawaves GmbH was founded as spin-off company from TUH. Our patented high-power ultrasound systems were and are developed on the basis of the wealth of knowledge acquired over many years. Ultrawaves is now the worldwide market leader for ultrasound applications in environmental engineering.
The BIOSONATOR is our new complete system consisting of a modular high-power ultrasound system, upstream a macerator and an eccentric screw pump as well as an intelligent control and automation technology with remote maintenance. As a plug and play system, the BIOSONATOR can be quickly and easily integrated into existing biogas plants.
=== VTA ===
{{Infobox provider-ultrasonication|Company=VTA Technologie GmbH|Country=Austria|Webpage=https://vta.cc/en|Technology name=VTA GSD|Power=3000-4000|Frequency=25|Processable volume=300-2500|Product=Dewatered sludge for efficient drying|Feedstock=Sewage sludge}}
VTA is an Austrian group which is successful all over the world. We develop and create innovative system products and technologies which set standards in the waste water and environmental engineering sector. These high-performance, cost-efficient and sustainable solutions are inspired by nature and its cycles.
Optimum sewage sludge treatment, stable digestion operation and reduction of costs – this is what reverse flow disintegration (GSD) with ultrasound, a patented process from VTA Technologie GmbH, has to offer. In VTA GSD, ultrasonic transducers digest the thickened sludge flowing through the disintegration reactor.
=== Weber ===
{{Infobox provider-ultrasonication|Company=Weber Ultrasonics / ENTEC|Country=Germany|Webpage=https://www.weber-entec.com/en|TRL=9|Technology name=DesiUS/BIOPUSH|Power=2000 W per unit|Frequency=22|Product=Disintegrated biomass for further processing|Feedstock=Waste water, slurry, maize, silage, grass, manure/GPS}}
Weber Entec GmbH & Co. KG is a subsidiary of Weber Ultrasonics AG, one of the world’s leading manufacturers of ultrasound components and ultrasonic welding equipment. Weber Entec concentrates on systems engineering and applications using ultrasound in the field of environmental engineering, especially ultrasonic treatment of biogenic materials, known as disintegration. Weber Entec specializes in disintegration with ultrasound for wastewater treatment and biogas plants.
Because of its broad range of services, the company is a one-stop source for manufacturing, plant construction, sales, system analysis and process optimisation.  Developed in a research project with the renowned Fraunhofer Institute, our subsidiary’s systems technology accelerates the decomposition of organic material. Today the Weber Entec technology is at work in biogas and water treatment plants all over the world. Customers benefit from efficient processes and a higher energy yield.


== Open access pilot and demo facility providers ==
== Open access pilot and demo facility providers ==

Latest revision as of 10:12, 7 March 2023

Technology
21-04-27 Tech4Biowaste rect-p.png
Technology details
Name: Ultrasonication
Category: Pre-processing (Physical processes and technologies), Post-processing (Physical processes and technologies)
Feedstock: Biowaste
Product: Biomass (dispersed, disrupted, emulsified, extracted, homogenised)

Ultrasonication is a physical treatment to disperse, disrupt, emulsify, extract, and/or homogenise biomass via the application of ultrasonic frequencies (>20 kHz). The propagation of sound waves through the biomass results in spontaneous formation and collapse of microsized cavities. This activity produces a hot-spot effect, resulting in high temperature and pressure gradients to form locally, while the overall conditions remain ambient. This effect can be used to break down morphologies, for example for the depolymerisation of lignocellulosic biowaste.[1]

Feedstock

Composition

The requirements on the composition of the feedstock may vary since ultrasonication can be utilised at various points in the value chain of biowaste valorisation.

Pre-treatment

Ultrasonication is often the first step of the pretreatment, although initial sizing may be required.

Process and technologies

During the ultrasonication treatment, ultrasound is transmitted through any physical medium by waves that compress and stretch the molecular spacing of the medium through which it passes[2]. The distance between the molecules will vary as they oscillate about their mean position[2]. When the negative pressure is large enough, the distance between the molecules of the liquid exceeds the minimum molecular distance required to hold the liquid intact, and then the liquid breaks down and voids (cavitation bubbles) are created[2].

The medium for ultrasonication can be water, an organic solvent, or a dilute acid or base.[1]

Schematic of bench and industrial-scale ultrasonic liquid processors
Schematic of bench and industrial-scale ultrasonic liquid processors produced by Industrial Sonomechanics, LLC

Product

Ultrasonication can be used to produce:

  • Emulsions (such as nanoparticles, nanoemulsions, nanocrystals, liposomes, wax emulsions)
  • Extracts from biomass (such as polysaccharides[3], oil, anthocyanins and antioxidants[4])
  • Purified wastewater

Furthermore, ultrasonication is also utilised in following processes:

  • Adhesive thinning
  • Cells disruption
  • Degassing liquids
  • Polymer and epoxy processing
  • Ultrasound assisted oxidative desulfurisation of crude oil[5]

Post-treatment

A common application for ultrasonication is breaking down the lignocellulosic structure. The available sugars can then be converted to products such as biofuels, for example by fermentation.[1]

Technology providers

Technology comparison
Company name Country Technology subcategory Technology name TRL Capacity [kg/h] Frequency [kHz] Power [W] Processable volume [L] Feedstock: Food waste Feedstock: Garden & park waste
Everywave Srl Italy - FLOW:WAVE® Tubular reactor 5 2000 20-40 2000-4000 4
Hielscher Ultrasonics GmbH Germany - UIP16000 9 - 18 40000 5
Doosan Enpure Limited United Kingdom - SonixTM - - 20 - -
Ultrawaves Germany - BIOSONATOR - 1980 20-1000 10000 20-50
VTA Austria - VTA GSD - - 25 3000-4000 300-2500
Weber Germany - DesiUS/BIOPUSH 9 - 22 2000 -

Everywave Srl

Ultrasonication provider
General information
Company: Everywave Srl Everywavelogo.png
Country: Italy
Contact: info@everywave.eu
Webpage: https://www.everywave.eu/en/
Technology and process details
Technology name: FLOW:WAVE® Tubular reactor Technology category: Pre-processing (Physical processes and technologies), Post-processing (Physical processes and technologies)
TRL: 5 Capacity: 2 tons/hour per single module kg·h-1
Frequency: 20/40 kHz Power: 2000/4000 W
Processable volume: 4 L Other: Continuous process
Feedstock and product details
Feedstock: By-products and biomasses (slurry, manure, sorghum, triticale, corn silage, other livestock waste, or residues from the agri-food industry, etc.) Product: emulsion, mixing, disintegration, sonochemistry, plant extraction, and bactericidal action.

Everywave Srl is a spin-off from UNITECH Srl that specializes in the research, development and production of solutions in the ultrasound technologies. The continuous and rapid technological evolution and the need for ever higher quality standards require the daily research and development of increasingly innovative solutions where quality and reliability play an absolutely vital role in all working processes. Everywave’s mission has always been to find ideas and improvement solutions in the field of ultrasound technologies, with continuous support to its customers in order to optimize their productivity and therefore their competitiveness.

Today, with a specialized biomass treatment plant, the company also produces biogas from the same by-products: a source that reduces the energy supply costs necessary for the company and generates a new source of income. We have designed and produced a special ultrasonic reactor which, integrated with specialized systems for shredding, pumping and process control, represents a solid and efficient technology for controlling and increasing the production yield of biogas.

Hielscher Ultrasonics GmbH

Ultrasonication provider
General information
Company: Hielscher Ultrasonics GmbH Hielscher.png
Country: Germany
Contact: info@hielscher.com
Webpage: www.hielscher.com
Technology and process details
Technology name: UIP16000 Technology category: Pre-processing (Physical processes and technologies), Post-processing (Physical processes and technologies)
TRL: 9 Capacity: kg·h-1
Frequency: 18 kHz Power: 40,000 W
Processable volume: 5 L Other: Biodiesel transesterification (12-50m³/h ) Emulsification (e.g. oil/water 6-32m³/h), Cell extraction (e.g. algae 1-12m³/h), Dispersion/deagglomeration (0.3-6m³/h), Wet milling (0.2-4m³/h)
Feedstock and product details
Feedstock: Biomass, 2-phase systems Product: Dispersion, Emulsion, Cell extract

Hielscher Ultrasonics specialises in the design and manufacturing of high power ultrasonic homogenisers for lab, bench-top and production level. Ultrasonic power is an effective and energy-efficient means to apply high shear and intense stress to liquids, powder/liquid mixtures and slurries. This makes it a strong alternative to high shear mixers, high pressure homogenisers and agitated bead mills. Hielscher ultrasonic devices are in use worldwide as laboratory mixers, high shear mixing equipment, full-size in-line homogenisers or particle mills. The applications include mixing, dispersing, particle size reduction, extraction and chemical reactions. Hielscher supply to various industry segments, such as nano-materials, paints & pigments, food & beverage, cosmetics, chemicals and fuels.

Doosan Enpure Limited

Ultrasonication provider
General information
Company: Doosan Enpure Limited 21-04-27 Tech4Biowaste rect-p.png
Country: United Kingdom
Contact:
Webpage: https://www.doosanenpure.com/
Technology and process details
Technology name: SonixTM Technology category: Pre-processing (Physical processes and technologies), Post-processing (Physical processes and technologies)
TRL: Capacity: 200 m3/d kg·h-1
Frequency: 20 kHz Power: W
Processable volume: L Other:
Feedstock and product details
Feedstock: Wastewater sludge, or any other biological or cellular material Product: Disintegrated material

Doosan Enpure Limited is a process engineering company specializing in water, wastewater and sludge treatment as well as waste-to-energy solutions with a global presence. We are a wholly-owned subsidiary of Doosan Heavy Industries & Construction, a global conglomerate in the power and water infrastructure sector, headquartered in South Korea.

Doosan Enpure provides a wide range of sludge treatment processes to meet all legislative requirements as well as maximising the recovery of energy and other useful components of the sludge.

Ultrawaves

Ultrasonication provider
General information
Company: ULTRAWAVES - Water- and Environmental Technologies GmbH 21-04-27 Tech4Biowaste rect-p.png
Country: Germany
Contact:
Webpage: https://ultrawaves.de/en/
Technology and process details
Technology name: BIOSONATOR Technology category: Pre-processing (Physical processes and technologies), Post-processing (Physical processes and technologies)
TRL: Capacity: 10 to 33 L/min or 0.6 to 2 m3/h biomass suspension kg·h-1
Frequency: 20-1000 kHz Power: 3000-10000 W
Processable volume: 20-50 L Other:
Feedstock and product details
Feedstock: Renewable raw materials, maize, green waste, slurry, municipal and industrial wastewater Product: Disintegrated biomass for further processing

ULTRAWAVES GmbH develops and markets innovative high-power ultrasonic systems for water and environmental engineering. Apart from the disintegration of biomass in wastewater treatment and biogas plants, the systems are also used in industrial applications. In 2001 Ultrawaves GmbH was founded as spin-off company from TUH. Our patented high-power ultrasound systems were and are developed on the basis of the wealth of knowledge acquired over many years. Ultrawaves is now the worldwide market leader for ultrasound applications in environmental engineering.

The BIOSONATOR is our new complete system consisting of a modular high-power ultrasound system, upstream a macerator and an eccentric screw pump as well as an intelligent control and automation technology with remote maintenance. As a plug and play system, the BIOSONATOR can be quickly and easily integrated into existing biogas plants.

VTA

Ultrasonication provider
General information
Company: VTA Technologie GmbH 21-04-27 Tech4Biowaste rect-p.png
Country: Austria
Contact:
Webpage: https://vta.cc/en
Technology and process details
Technology name: VTA GSD Technology category: Pre-processing (Physical processes and technologies), Post-processing (Physical processes and technologies)
TRL: Capacity: kg·h-1
Frequency: 25 kHz Power: 3000-4000 W
Processable volume: 300-2500 L Other:
Feedstock and product details
Feedstock: Sewage sludge Product: Dewatered sludge for efficient drying

VTA is an Austrian group which is successful all over the world. We develop and create innovative system products and technologies which set standards in the waste water and environmental engineering sector. These high-performance, cost-efficient and sustainable solutions are inspired by nature and its cycles.

Optimum sewage sludge treatment, stable digestion operation and reduction of costs – this is what reverse flow disintegration (GSD) with ultrasound, a patented process from VTA Technologie GmbH, has to offer. In VTA GSD, ultrasonic transducers digest the thickened sludge flowing through the disintegration reactor.

Weber

Ultrasonication provider
General information
Company: Weber Ultrasonics / ENTEC 21-04-27 Tech4Biowaste rect-p.png
Country: Germany
Contact:
Webpage: https://www.weber-entec.com/en
Technology and process details
Technology name: DesiUS/BIOPUSH Technology category: Pre-processing (Physical processes and technologies), Post-processing (Physical processes and technologies)
TRL: 9 Capacity: kg·h-1
Frequency: 22 kHz Power: 2000 W per unit W
Processable volume: L Other:
Feedstock and product details
Feedstock: Waste water, slurry, maize, silage, grass, manure/GPS Product: Disintegrated biomass for further processing

Weber Entec GmbH & Co. KG is a subsidiary of Weber Ultrasonics AG, one of the world’s leading manufacturers of ultrasound components and ultrasonic welding equipment. Weber Entec concentrates on systems engineering and applications using ultrasound in the field of environmental engineering, especially ultrasonic treatment of biogenic materials, known as disintegration. Weber Entec specializes in disintegration with ultrasound for wastewater treatment and biogas plants.

Because of its broad range of services, the company is a one-stop source for manufacturing, plant construction, sales, system analysis and process optimisation.  Developed in a research project with the renowned Fraunhofer Institute, our subsidiary’s systems technology accelerates the decomposition of organic material. Today the Weber Entec technology is at work in biogas and water treatment plants all over the world. Customers benefit from efficient processes and a higher energy yield.

Open access pilot and demo facility providers

Currently no providers have been identified.

Patents

Currently no patents have been identified.

References

  1. a b c Preeti Bhagwan Subhedar, 2016: Use of Ultrasound for Pretreatment of Biomass and Subsequent Hydrolysis and Fermentation. Biomass fractionation technologies for a lignocellulosic feedstock based biorefinery. (Ed.). Elsevier, Amsterdam, Netherlands.
  2. a b c Hugo Miguel Santos, Carlos Lodeiro, and José-Luis Capelo-Martínez, 2008: The Power of Ultrasound. Ultrasound in Chemistry: Analytical Applications. José-Luis Capelo-Martínez (Ed.). Wiley‐VCH Verlag GmbH & Co. KGaA, Weinheim, Germany.
  3. , 2017-09-01: Polysaccharides from macroalgae: Recent advances, innovative technologies and challenges in extraction and purification. Food Research International, Vol. 99, 1011–1020. doi: https://doi.org/10.1016/j.foodres.2016.11.016
  4. , 2013-09-01: Effect of ultrasound frequency on antioxidant activity, total phenolic and anthocyanin content of red raspberry puree. Ultrasonics Sonochemistry, Vol. 20, (5), 1316–1323. doi: https://doi.org/10.1016/j.ultsonch.2013.01.020
  5. , 2020-05-01: Study on ultrasound-assisted oxidative desulfurization for crude oil. Ultrasonics Sonochemistry, Vol. 63, 104946. doi: https://doi.org/10.1016/j.ultsonch.2019.104946